翻译.Solid phase extraction (SPE) as a preconcentration-separa

翻译.
Solid phase extraction (SPE) as a preconcentration-separation technique coupled with flame atomic absorption spectrometric
(FAAS) has been applied for determination of trace heavy metals in water (tap, river, sea and industrial), soil, food, pharmaceuti- cal, marine sediment and biological samples [1–7]. FAAS is one of the most popular techniques for determination of metal ions because of its high specificity and low cost. However its sensitiv- ity is usually insufficient for determination of trace metal ions in environmental samples. In order to overcome this problem and pre- vent interference effects, the method usually requires an efficient preconcentration step [8,9].
Many methods, either on-line or batch systems, have been developed for the preconcentration of trace metals from various samples, including coprecipitation [10–13], liquid–liquid extrac- tion [14–17], solid phase extraction [18–20] and cloud point extraction [21–24]. Among these techniques, SPE is one of the most important preconcentration methodologies because of its simplicity, flexibility to choose the solid phase, high preconcentra- tion factor, low consumption of the organic solvents, low cost and extraction time for sample preparation [25–32].
wendyedwin 1年前 已收到2个回答 举报

糯糯_心 幼苗

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作为富集-分离技术的固相萃取(SPE)和空气-乙炔原子吸收光谱法(FAAS)一起已经被用于确定水(水龙头、河流、大海和产业界)、土壤、食品、药品、海洋沉积物及生物样本中的痕量重金属【1-7】.FAAS是用于确定金属离子最普及的技术之一,因为它具有高的特异性和低的成本.然而它的灵敏度对于确定环境样本中的痕量金属离子来说却是不够的.为了克服这一问题和防止干扰的影响,这种方法通常需要有高效的预富集步骤【8,9】.
为了从各种不同样本中富集痕量金属,已开发了很多种方法,既有在线的,也有批处理系统的,其中包括共沉淀法【10-13】、液-液萃取法【14-17】,固相萃取法【18-20】和浊点萃取法【21-24】.在这些技术中,SPE是一种最重要的富集方法,因为它选择固相比较简单、灵活,高的富集倍数,低的有机溶剂消耗量,样本制备的低成本和萃取时间【25-32】.

1年前

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但愿能活五百年 幼苗

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固相萃取(萃取)作为富集分离技术,加上火焰原子吸收光谱
(火焰原子吸收光谱法)已用于测定痕量重金属的水(自来水,河,海,工业) ,土壤,食品,制药加州,海洋沉积物和生物样品[ 1-7 ] 。火焰原子吸收光谱法是一种最流行的技术测定金属离子由于其特异性高,成本低等优点。然而其敏感性通常是不够的测定痕量金属离子在环境样品。为了克服这一问题,并预先发泄干扰效应,这种方法通常需要一个有效的富集步...

1年前

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